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111.
S.H. Momeni‐Masuleh A. Malek 《Numerical Methods for Partial Differential Equations》2007,23(5):1139-1148
This research aims to develop a time‐dependent pseudospectral‐finite difference scheme for solving a 3D dual‐phase‐lagging heat transport equation in a submicroscale thin film. The scheme uses periodic pseudospectral discretization in space and a fully second‐order finite difference discretization in time. The three consecutive time steps model is then solved explicitly, by using a preconditioned conjugate gradient method. The scheme is illustrated by an example which is used to investigate the heat transfer in a gold submicroscale thin film. Comparisons are made with available literature. © 2007 Wiley Periodicals, Inc. Numer Methods Partial Differential Eq, 2007 相似文献
112.
Mohsen Timoumi 《Reports on Mathematical Physics》2004,54(1):1-21
In this paper we study in some particular cases, the existence and multiplicity of closed trajectories of a relativistic particle moving in some electromagnetic fields. To solve this problem, we use Hamiltonian systems and variational methods. 相似文献
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115.
Mohsen Esmaeilpour Jaber Javidi Elahe Rezaei 《Phosphorus, sulfur, and silicon and the related elements》2017,192(5):530-537
An efficient and environment friendly process for the synthesis of α-aminophosphonates has been devised. Through a one-pot three-component condensation of various aldehydes, amines, and triethyl phosphite in the presence of Fe3O4@SiO2-imid-PMAn nanoparticles as magnetic catalysts under solvent-free conditions and ultrasonic irradiation, α-aminophosphonates were obtained with excellent yields. The reactions under solvent-free conditions at room temperature are compared with the ultrasonic-assisted reactions. This new procedure has notable advantages such as short reaction time, excellent yields, easy purification, and the absence of any tedious workup or purification. The aforementioned catalyst could be easily recovered by an external magnetic field and can be reused for six consecutive reaction cycles without significant loss of activity. In addition, SEM and DLS of the catalyst after the reaction cycle were investigated. 相似文献
116.
Mohsen Esmaeilpour Jaber Javidi Farzaneh Dehghani Saeed Zahmatkesh 《Research on Chemical Intermediates》2017,43(1):163-185
An efficient, green and eco-friendly protocol has been developed for the synthesis of 2,4,5-trisubstituted and 1,2,4,5-tetrasubstituted imidazoles via one-pot condensation reaction using Dendrimer-PWAn as catalyst under solvent-free conditions or ultrasonic irradiation in excellent yields. The reactions under conventional heating conditions were compared with the ultrasonic-assisted reactions. The operational simplicity, practicability and applicability of this protocol to various substrates make it an interesting alternative to previous procedures. The present methodology offers several advantages such as excellent yields, short reaction times, a cleaner reaction, and the absence of any tedious work-up or purification. The catalyst is easily separated from the products by filtration and also exhibits remarkable reusable activity. SEM, BET and DLS of the catalyst were also investigated after each reaction cycle. 相似文献
117.
Mohsen Keyvanfard Nazila Najjarian Khadijeh Alizad 《Journal of Analytical Chemistry》2017,72(10):1045-1050
In this study, we describe the application of carbon paste electrode modified with multiwall carbon nanotubes as a voltammetric sensor for determination of penicillamine (PA) in the presence of chlorpromazine as a mediator. This modified electrode showed very efficient electrocatalytic activity for the anodic oxidation of PA. The peak current of linear sweep voltammograms of PA increased linearly with it’s concentration in the range of 0.5–500 μM PA. The detection limit for PA was 0.2 μM. The RSDs for 1.0 and 10.0 μM PA were 1.1 and 1.7%, respectively. The proposed sensor was successfully applied for the determination of PA in human urine and tablet. 相似文献
118.
Mohsen Padervand Solmaz Ghaffari Mahdieh Mohammad Nejad 《Journal of Analytical Chemistry》2017,72(5):567-574
Sunitinib malate, as an anticancer compound and a multi-targeted tyrosine-kinase inhibitor for treatment of glioma, was comprehensively studied by using different liquid chromatography methods. Since sunitinib malate shows Z-E isomerism, various reverse phase high performance liquid chromatography (RP-HPLC) programs were designed to access quantitative determination and good separation of Z-E stereoisomers. Moreover, some impurities including N-oxide and impurity B were to be separated from the main isomer with acceptable resolution. In the present work, different RP-HPLC programs were developed in which the type of mobile phase, flow rate, pH, and temperature were optimized to reach the best analysis conditions and control the rate of Z to E conversion. In addition, the effect of some operational parameters during the solution preparation including initial concentration of the analyte, temperature, pH, and type of solvent on the stability of Z isomer were investigated. The opted conditions for quantitative analysis were C8-Hector column as stationary phase, methanol as solvent, ammonium acetate buffer containing triethylamine as mobile phase, the pH of mobile phase of 8.5, the flow rate of 1.0 mL/min, and detection at 425 nm. In this situation the peaks of E and Z isomers were at 16.3 and 19.7 min. Full validation of the designed method was done based on ICH guidelines. 相似文献
119.
We present a preconditioner for saddle point problems. The proposed preconditioner is extracted from a stationary iterative method which is convergent under a mild condition. Some properties of the preconditioner as well as the eigenvalues distribution of the preconditioned matrix are presented. The preconditioned system is solved by a Krylov subspace method like restarted GMRES. Finally, some numerical experiments on test problems arisen from finite element discretization of the Stokes problem are given to show the effectiveness of the preconditioner. 相似文献
120.
The present paper deals with the study of semilinear and non-homogeneous Schrödinger equations on a manifold with conical singularity. We provide a suitable constant by Sobolev embedding constant and for p ∈ (2, 2?) with respect to non-homogeneous term g(x) ∈ L 2 n/2 (B), which helps to find multiple solutions of our problem. More precisely, we prove the existence of two solutions to the problem 1.1 with negative and positive energy in cone Sobolev space H 2,0 1,n/2 (B). Finally, we consider p = 2 and we prove the existence and uniqueness of Fuchsian-Poisson problem. 相似文献